1-氯丙烯(顺反混合物)合成路线 （共 34 条）
反应条件
sodium chloride; sodium hydroxide T=81°C;
参考文献
DOW GLOBAL TECHNOLOGIES, LLC; TIRTOWIDJOJO, Max Markus; FISH, Barry
Patent: WO2013/74414 A1, 2013 ;
Location in patent: Paragraph 0059-0061 ;
反应条件
sodium hydroxide T=125°C; unter Druck;
参考文献
Dow Chem.Co.
Patent: US2543648 , 1943 ;
反应条件
tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 0.166667 h; Ambient temperature;
参考文献
Guibe, Francois; Zigna, Anne-Marie; Balavoine, G.
Journal of Organometallic Chemistry, 1986 , vol. 306, p. 257 - 266
反应条件
tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 0.166667 h; Ambient temperature;
参考文献
Guibe, Francois; Zigna, Anne-Marie; Balavoine, G.
Journal of Organometallic Chemistry, 1986 , vol. 306, p. 257 - 266
反应条件
tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 0.166667 h;
参考文献
Guibe, Francois; Zigna, Anne-Marie; Balavoine, G.
Journal of Organometallic Chemistry, 1986 , vol. 306, p. 257 - 266
反应条件
lithium aluminium tetrahydride; di-isopropyl ether
参考文献
Hatch; Perry
Journal of the American Chemical Society, 1949 , vol. 71, p. 3262
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride T=105°C; 1 h;
参考文献
Guibe, Francois; Zigna, Anne-Marie; Balavoine, G.
Journal of Organometallic Chemistry, 1986 , vol. 306, p. 257 - 266
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride T=105°C; 1 h;
参考文献
Guibe, Francois; Zigna, Anne-Marie; Balavoine, G.
Journal of Organometallic Chemistry, 1986 , vol. 306, p. 257 - 266
反应条件
2,2'-azo-bisisobutyronitrile; QN3 T=105°C; 1 h;
参考文献
Guibe, Francois; Zigna, Anne-Marie; Balavoine, G.
Journal of Organometallic Chemistry, 1986 , vol. 306, p. 257 - 266
反应条件
in n-heptane T=21.9°C; Irradiation; Quantum yieldThermodynamic data;
参考文献
LaVilla, Joseph A.; Goodman, Joshua L.
Journal of the American Chemical Society, 1989 , vol. 111, # 17 p. 6877 - 6878
