N-羟基-4-硝基苯甲酰胺合成路线 （共 20 条）
反应条件
N-bromosuccinmide; hydroxylamine hydrochloride; triphenylphosphine in triethylamine; acetonitrile T=20°C; Mitsunobu reaction; 2 h;
参考文献
Dhuru, Sameer P.; Salunkhe, Manikrao M.
Journal of the Chinese Chemical Society, 2000 , vol. 47, # 4 B p. 1007 - 1008
反应条件
potassium hydroxide; hydroxylamine hydrochloride in methanol 36 h; Ambient temperature;
参考文献
Liguori, Angelo; Sindona, Giovanni; Romeo, Giovanni; Uccella, Nicola
Synthesis, 1987 , # 2 p. 168
反应条件
hydroxylamine hydrochloride; potassium hydroxide in methanol 24 h; Reflux;
参考文献
Kreye, Oliver; Wald, Sarah; Meier, Michael A. R.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 1 p. 81 - 86
反应条件
Nafion-H in isopropyl alcohol 20 h; Heating;
参考文献
Couturier, Michel; Tucker, John L.; Proulx, Caroline; Boucher, Ghislain; Dube, Pascal; Andresen, Brian M.; Ghosh, Arun
Journal of Organic Chemistry, 2002 , vol. 67, # 14 p. 4833 - 4838
反应条件
hydroxylamine hydrochloride; sodium carbonate in diethyl ether; water
参考文献
Werner; Skiba
Chemische Berichte, 1899 , vol. 32, p. 1658
Full Text Show Details
Holleman
Recueil des Travaux Chimiques des Pays-Bas, 1897 , vol. 16, p. 186
反应条件
(hydroxy(tosyloxy)iodo)benzene in dimethyl sulfoxide T=20 - 80°C; 1.5 h;
参考文献
Ghosh, Harisadhan; Baneerjee, Arghya; Rout, Saroj Kumar; Patel, Bhisma K.
Arkivoc, 2011 , vol. 2011, # 2 p. 209 - 216
反应条件
hydroxylamine; sodium carbonate
参考文献
Werner; Skiba
Chemische Berichte, 1899 , vol. 32, p. 1658
Full Text Show Details
Holleman
Recueil des Travaux Chimiques des Pays-Bas, 1897 , vol. 16, p. 186
反应条件
hydroxylamine in water; dimethyl sulfoxide T=25°C; Rate constant;
参考文献
Um, Ik-Hwan; Chung, Eun-Kyung; Lee, So-Mi
Canadian Journal of Chemistry, 1998 , vol. 76, # 6 p. 729 - 737
反应条件
potassium carbonate in dimethyl sulfoxide T=90°C; Lossen rearrangement; 9 h;
参考文献
Hoshino, Yujiro; Okuno, Moriaki; Kawamura, Eri; Honda, Kiyoshi; Inoue, Seiichi
Chemical Communications, 2009 , # 17 p. 2281 - 2283
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine Lossen Rearrangement; 20 h; RefluxGreen chemistry;
参考文献
Kreye, Oliver; Wald, Sarah; Meier, Michael A. R.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 1 p. 81 - 86
