2,2'-联吡啶-4-甲腈合成路线 (共 3 条)
反应条件
phosphorus trichoride in dichloromethane T=60°C; 1 h; Inert atmosphere;
参考文献
Duric, Sasa; Tzschucke, C. Christoph
Organic Letters, 2011 , vol. 13, # 9 p. 2310 - 2313
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; Negishi reaction; 18 h;
参考文献
Siu, Jason; Baxendale, Ian R.; Lewthwaite, Russell A.; Ley, Steven V.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 17 p. 3140 - 3160
反应条件
1: tri-tert-butyl phosphine; palladium diacetate; potassium carbonate / toluene / 24 h / 120 °C / Inert atmosphere 2: phosphorus trichoride / dichloromethane / 1 h / 60 °C / Inert atmosphere View Scheme
参考文献
Duric, Sasa; Tzschucke, C. Christoph
Organic Letters, 2011 , vol. 13, # 9 p. 2310 - 2313