反应条件
in neat (no solvent) High Pressure; pressure react. of dry HCl and Ph4Ge in autoclave (molar ratio Ph4Ge/HCl = 6.7), initial pressure 44 atm, 8h; rinsing react. mixt. with pentane into retort; evapn.; addn. of pentane; cooling to -15°C; crystn. overnight; filtration; recrystn. (petroleum ether);
参考文献
Zeitschrift fuer Naturforschung, B: Chemical Sciences, , vol. 42, # 3 p. 323 - 329
