(4-溴苯基乙炔基)三甲基硅烷合成路线 （共 34 条）
参考文献
Tetrahedron Letters, , vol. 39, # 26 p. 4745 - 4748
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Heating;
参考文献
Pena, Miguel A.; Perez Sestelo, Jose; Sarandeses, Luis A.
Synthesis, 2005 , # 3 art. no. Z14204SS, p. 485 - 492
反应条件
n-butyllithium; tri-isopropoxy-borane in tetrahydrofuran; hexane T=-60°C;
参考文献
Newby, James A.; Huck, Lena; Blaylock, D. Wayne; Witt, Paul M.; Ley, Steven V.; Browne, Duncan L.
Chemistry - A European Journal, 2014 , vol. 20, # 1 p. 263 - 271
反应条件
1: (4-bromophenylethynyl)trimethylsilane With potassium carbonate in methanol 5 h; 2: With n-butyllithium in tetrahydrofuran T=-78°C; 3: dimethylmono-chlorosilane in tetrahydrofuran
参考文献
Wang, Fei; Kaafarani, Bilal R.; Neckers, Douglas C.
Macromolecules, 2003 , vol. 36, # 22 p. 8225 - 8230
反应条件
1: [1,3-bis(diphenylphosphino) propane] dichloronickel(II) / diethyl ether / 24 h / Reflux 2: potassium carbonate / tetrahydrofuran; methanol / 20 °C / Inert atmosphere View Scheme
参考文献
Meng, Qing; Jiang, Lang; Wei, Zhongming; Wang, Chengliang; Zhao, Huaping; Li, Hongxiang; Xu, Wei; Hu, Wenping
Journal of Materials Chemistry, 2010 , vol. 20, # 48 p. 10931 - 10935
反应条件
toluene-4-sulfonic acid in neat (no solvent) T=60 - 140°C; 22 h; Green chemistry; regioselective reaction;
参考文献
Gao, Qi; Bao, Fang-Ping; Feng, Xiao-Jing; Pan, Ying-Ming; Wang, Heng-Shan; Li, Dian-Peng
Arkivoc, 2013 , vol. 2013, # 3 p. 49 - 60
反应条件
potassium carbonate in methanol; dichloromethane T=23°C; 5 h;
参考文献
Pearson, Darren L.; Tour, James M.
Journal of Organic Chemistry, 1997 , vol. 62, # 5 p. 1376 - 1387
反应条件
potassium carbonate T=120 - 130°C; 0.25 h; microwave irradiation;
参考文献
Wettergren, Jenny; Minidis, Alexander B. E.
Tetrahedron Letters, 2003 , vol. 44, # 41 p. 7611 - 7612
反应条件
1: potassium carbonate / methanol; dichloromethane / 20 °C / Inert atmosphere 2: C27H34Cl3CuN2; sodium t-butanolate; tert-butyl alcohol / tetrahydrofuran; hexane / 20 h / 50 °C / Inert atmosphere View Scheme
参考文献
Semba, Kazuhiko; Fujihara, Tetsuaki; Xu, Tinghua; Terao, Jun; Tsuji, Yasushi
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 8 p. 1542 - 1550
反应条件
iodine; tert.-butyl lithium T=-78°C;
参考文献
Blakskjaer, Peter; Gothelf, Kurt V.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 18 p. 3442 - 3447
