2,4-二氯-6-三氟甲基嘧啶合成路线 （共 16 条）
反应条件
tri(n-propyl)amine; trichlorophosphate 3 h; Heating;
参考文献
Gershon, Herman; Grefig, Anthony T.; Clarke, Donald D
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 1243 - 1247
反应条件
hydrogenchloride in trichlorophosphate T=15 - 20°C;
参考文献
Gershon; Grefig; Scala
Journal of Heterocyclic Chemistry, 1983 , vol. 20, # 1 p. 219 - 223
反应条件
trichlorophosphate; N,N-diethylaniline 3 h; Heating;
参考文献
Gershon; Grefig; Scala
Journal of Heterocyclic Chemistry, 1983 , vol. 20, # 1 p. 219 - 223
反应条件
1: 62 percent / ethanol / Ambient temperature; overnight 2: 63 percent / conc. HCl / 64 h / Heating 3: 46 percent / phosphorus oxychloride, N,N-dimethylaniline / 3 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 21, p. 1161 - 1167
反应条件
1: 87 percent / NaOH / H2O / 1) RT, 3 h; 2) reflux, 5 min 2: 79 percent / 10 percent HCl / 8 h / Heating 3: 1) POCl3; 2) PCl5 / 1) reflux, overnight; 2) reflux, overnight View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 20, # 1 p. 219 - 223
反应条件
trichlorophosphate 3 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 21, p. 1161 - 1167
反应条件
phosphorus pentachloride; trichlorophosphate 1) reflux, overnight; 2) reflux, overnight; Yield given. Multistep reaction;
参考文献
Gershon; Grefig; Scala
Journal of Heterocyclic Chemistry, 1983 , vol. 20, # 1 p. 219 - 223
反应条件
N,N-dimethyl-aniline; trichlorophosphate 3 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 21, p. 1161 - 1167
反应条件
1: 63 percent / conc. HCl / 64 h / Heating 2: 46 percent / phosphorus oxychloride, N,N-dimethylaniline / 3 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 21, p. 1161 - 1167
反应条件
1: 79 percent / 10 percent HCl / 8 h / Heating 2: 1) POCl3; 2) PCl5 / 1) reflux, overnight; 2) reflux, overnight View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 20, # 1 p. 219 - 223
