1-(3-氟-4-硝基苯基)甲胺合成路线 (共 3 条)
反应条件
ammonium acetate; molecular sieve; sodium cyanoborohydride in methanol 24 h;
参考文献
Rao, A V Rama; Reddy, K Laxma; Rao, A Srinivasa
Tetrahedron Letters, 1994 , vol. 35, # 45 p. 8465 - 8468
反应条件
borane-THF in tetrahydrofuran T=0 - 20°C; 16 h;
参考文献
Therrien, Eric; Larouche, Guillaume; Manku, Sukhdev; Allan, Martin; Nguyen, Natalie; Styhler, Sylvia; Robert, Marie-France; Goulet, Anne-Christine; Besterman, Jeffrey M.; Nguyen, Hannah; Wahhab, Amal
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 23 p. 6725 - 6732
反应条件
1: 1.) chromium trioxide, sulfuric acid; 2.) sulfuric acid / 1.) acetic anhydride, 0 degC, 3 h; 2.) ethanol, water, 1 h 2: 61 percent / ammonium acetate, sodium cyanoborohydride, mol. sieves / methanol / 24 h View Scheme
参考文献
Rao, A V Rama; Reddy, K Laxma; Rao, A Srinivasa
Tetrahedron Letters, 1994 , vol. 35, # 45 p. 8465 - 8468