反应条件
tert.-butyl lithium in diethyl ether
-78°C, molar ratio of starting materials is 1:1, formation of the intermediate is very slow, LiCl elimination is fast, formed stannene reacts with starting (CH3)3CLi, thus the stannene can isolated (same results obtained in THF and THF/Et2O); not isolated;
参考文献
Anselme, G.; Couret, C.; Escudie, J.; Richelme, S.; Satge, J.
Journal of Organometallic Chemistry, 1991 , vol. 418, # 2-3 p. 321 - 328
