1.1: n-BuLi / tetrahydrofuran; hexane / 2 h / -60 °C
1.2: CeCl3 / tetrahydrofuran; hexane / 1 h / -60 °C
1.3: tetrahydrofuran; hexane / -60 - 20 °C
2.1: 0.14 g / p-TsOH / toluene / 12 h / Heating
View Scheme
参考文献
Klokkenburg, Mark; Lutz, Martin; Spek, Anthony L.; Van der Maas, John H.; Van Walree, Cornelis A.
Chemistry - A European Journal, 2003 , vol. 9, # 15 p. 3544 - 3554
1.1: n-BuLi / tetrahydrofuran; hexane / 2 h / -60 °C
1.2: CeCl3 / tetrahydrofuran; hexane / 1 h / -60 °C
1.3: tetrahydrofuran; hexane / -60 - 20 °C
2.1: 0.14 g / p-TsOH / toluene / 12 h / Heating
View Scheme
参考文献
Klokkenburg, Mark; Lutz, Martin; Spek, Anthony L.; Van der Maas, John H.; Van Walree, Cornelis A.
Chemistry - A European Journal, 2003 , vol. 9, # 15 p. 3544 - 3554
