4-(甲磺酰甲基)苯甲酸甲酯合成路线 (共 5 条)
反应条件
hydrogenchloride in 4-(dicyanomethylene)-2-methyl-6-(4-dimethylaminostyryl)-4H-pyran
参考文献
The Dupont Merck Pharmaceutical Company
Patent: US5879657 A1, 1999 ;
反应条件
hydrogenchloride in 4-(dicyanomethylene)-2-methyl-6-(4-dimethylaminostyryl)-4H-pyran
参考文献
Bristol-Myers Squibb Pharma Company
Patent: EP1293214 A2, 2003 ;
反应条件
dihydrogen peroxide; acetic acid 1 h; Heating;
参考文献
Chand, Pooran; Babu, Yarlagadda S.; Bantia, Shanta; Chu, Naiming; Cole, L. Brent; Kotian, Pravin L.; Laver, W. Graeme; Montgomery, John A.; Pathak, Ved P.; Petty, Sandra L.; Shrout, David P.; Walsh, David A.; Walsh, Gerald M.
Journal of Medicinal Chemistry, 1997 , vol. 40, # 25 p. 4030 - 4052
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane Ambient temperature;
参考文献
Chaudhari, Umesh V.; Deota, Pradeep T.
Organic Preparations and Procedures International, 2012 , vol. 44, # 4 p. 381 - 386
反应条件
1: 72 percent / dimethylformamide / 24 h / 20 °C 2: 69 percent / aq. H2O2; glacial acetic acid / 1 h / Heating View Scheme
参考文献
Chand, Pooran; Babu, Yarlagadda S.; Bantia, Shanta; Chu, Naiming; Cole, L. Brent; Kotian, Pravin L.; Laver, W. Graeme; Montgomery, John A.; Pathak, Ved P.; Petty, Sandra L.; Shrout, David P.; Walsh, David A.; Walsh, Gerald M.
Journal of Medicinal Chemistry, 1997 , vol. 40, # 25 p. 4030 - 4052