1,1-二甲基丙-2-炔基乙酸酯合成路线 （共 37 条）
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=45°C; 0.5 h;
参考文献
Ruitenberg, K.; Kleijn, H.; Westmijze, H.; Meijer, J.; Vermeer, P.
Recueil: Journal of the Royal Netherlands Chemical Society, 1982 , vol. 101, # 11 p. 405 - 409
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=45°C; 0.5 h;
参考文献
Ruitenberg, K.; Kleijn, H.; Westmijze, H.; Meijer, J.; Vermeer, P.
Recueil: Journal of the Royal Netherlands Chemical Society, 1982 , vol. 101, # 11 p. 405 - 409
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=45°C; 0.5 h;
参考文献
Ruitenberg, K.; Kleijn, H.; Westmijze, H.; Meijer, J.; Vermeer, P.
Recueil: Journal of the Royal Netherlands Chemical Society, 1982 , vol. 101, # 11 p. 405 - 409
反应条件
tetrakis(triphenylphosphine) palladium(0); zinc(II) chloride
2) THF, 25 deg C; Yield given. Multistep reaction;
参考文献
Elsevier, Cornelis J.; Kleijn, Henk; Ruitenberg, Klaas; Vermeer, Peter
Journal of the Chemical Society, Chemical Communications, 1983 , # 24 p. 1529 - 1530
反应条件
dichloro bis(acetonitrile) palladium(II) in acetonitrile
T=60°C; 17 h; Further byproducts given;
参考文献
Rautenstrauch, Valentin
Tetrahedron Letters, 1984 , vol. 25, # 35 p. 3845 - 3846
反应条件
dichloro bis(acetonitrile) palladium(II) in acetonitrile
T=60°C; 17 h; Further byproducts given;
参考文献
Rautenstrauch, Valentin
Tetrahedron Letters, 1984 , vol. 25, # 35 p. 3845 - 3846
反应条件
dichloro bis(acetonitrile) palladium(II) in acetonitrile
T=60°C; 19 h; Mechanism;
参考文献
Rautenstrauch, Valentin
Tetrahedron Letters, 1984 , vol. 25, # 35 p. 3845 - 3846
反应条件
1: dioxane
2: aq.-ethanolic KOH-solution
View Scheme
参考文献
Nasarow et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 1859,1862; engl. Ausg. S. 1829, 1835
Engl. Ausg., 1959 , vol. 29, p. 1829,1835
反应条件
copper(l) chloride in tetrahydrofuran
2 h; Heating;
参考文献
Gabriele, Bartolo; Plastina, Pierluigi; Salerno, Giuseppe; Mancuso, Raffaella; Costa, Mirco
Organic Letters, 2007 , vol. 9, # 17 p. 3319 - 3322
反应条件
1,1-dimethylethylmagnesium chloride; magnesium bromide in diethyl ether
参考文献
Coulomb,F. et al.
Bulletin de la Societe Chimique de France, 1973 , p. 3352 - 3359
