反应条件
Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '147733', constants.ctx, '0')">Indole-3-propionic acid</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1209227', constants.ctx, '0')">n-butyllithium</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a>; <a href="#" onclick="return RXDsubstances(event, this, '1730733', constants.ctx, '0')">hexane</a> <br />T=-78°C; 0.0833333 h; Inert atmosphere; <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '385668', constants.ctx, '0')">pivaloyl chloride</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a>; <a href="#" onclick="return RXDsubstances(event, this, '1730733', constants.ctx, '0')">hexane</a> <br />T=-78 - -20°C; 0.75 h; Inert atmosphere; <br />
参考文献
Ruiz, Miriam; Lopez-Alvarado, Pilar; Menendez, J. Carlos Organic and Biomolecular Chemistry, 2010 , vol. 8, # 20 p. 4521 - 4523