N,N″-二-Z-二亚乙基三胺合成路线 (共 5 条)
反应条件
triethylamine in dichloromethane T=-20 - 22°C; 12 h;
参考文献
SCHERING AKTIENGESELLSCHAFT
Patent: EP946525 B1, 2004 ;
Location in patent: Page 17 ;
反应条件
in N,N-dimethyl-formamide T=20°C;
参考文献
Pittelkow, Michael; Lewinsky, Rasmus; Christensen, Jorn Bolstad
Synthesis, 2002 , # 15 p. 2195 - 2202
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane T=50°C;
参考文献
McCarthy, Orla; Musso-Buendia, Alex; Kaiser, Marcel; Brun, Reto; Ruiz-Perez, Luis M.; Johansson, Nils Gunnar; Pacanowska, Dolores Gonzalez; Gilbert, Ian H.
European Journal of Medicinal Chemistry, 2009 , vol. 44, # 2 p. 678 - 688
反应条件
in dichloromethane T=-40°C;
参考文献
Adamczyk, Maciej; Fishpaugh, Jeffrey R.; Heuser, Kevin J.
Organic Preparations and Procedures International, 1998 , vol. 30, # 3 p. 339 - 348
反应条件
in dichloromethane T=5 - 7°C; 0.5 h;
参考文献
Sosnovsky, George; Lukszo, Jan
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1994 , vol. 49, # 11 p. 1580 - 1585