6-氯-3,4-亚甲基二氧苯甲醛合成路线 （共 8 条）
反应条件
bis(collidine)bromine(I) hexafluorophosphate in dichloromethane T=20°C; 10 h;
参考文献
Tetrahedron Letters, , vol. 41, # 46 p. 8881 - 8885
反应条件
sulfuryl dichloride T=20°C;
参考文献
Chemische Berichte, , vol. 43, p. 2605
反应条件
1: aq. NaOH solution 2: water; hydrobromic acid View Scheme
参考文献
Naik; Wheeler
Journal of the Chemical Society, 1938 , p. 1780,1782
反应条件
1: aq. NaOH solution 2: benzene; hydrogen chloride View Scheme
参考文献
Naik; Wheeler
Journal of the Chemical Society, 1938 , p. 1780,1782
参考文献
Barthel; Alexander
Journal of Organic Chemistry, 1958 , vol. 23, p. 1012
反应条件
tris-(dibenzylideneacetone)dipalladium(0); KF*2H2O; [(t-Bu)3PH]BF4 in tetrahydrofuran
Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Xia, Ying; Liu, Zhenxing; Xiao, Qing; Qu, Peiyuan; Ge, Rui; Zhang, Yan; Wang, Jianbo
Angewandte Chemie - International Edition, 2012 , vol. 51, # 23 p. 5714 - 5717
反应条件
sulfuric acid; acetic anhydride
参考文献
Parijs
Recueil des Travaux Chimiques des Pays-Bas, 1930 , vol. 49, p. 33,41
反应条件
pyridine; acetic anhydride; potassium carbonate
T=180°C; Erwaermen des Reaktionsprodukts mit Chlorwasserstoff enthaltendem Aethanol;
参考文献
Gertler et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 327
