1-甲基-4-(1-甲基丙基)苯合成路线 （共 47 条）
反应条件
1: sec.-butyl chloride With [1,3-bis(3,5-di-tert-butyl-2-hydroxybenzyl)benzimidazolium][FeCl4] in diethyl ether T=0°C; 0.0333333 h; Schlenk techniqueInert atmosphere; 2: (4-Methylphenyl)-magnesium bromide in diethyl ether T=0 - 30°C; 2 h; Schlenk techniqueInert atmosphere; Temperature;
参考文献
Xia, Chong-Liang; Xie, Cun-Fei; Wu, Yu-Feng; Sun, Hong-Mei; Shen, Qi; Zhang, Yong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 46 p. 8135 - 8144
反应条件
ethene; sodium T=185°C; Reagens 4: Anthracen;
参考文献
Pines; Schaap
Journal of the American Chemical Society, 1958 , vol. 80, p. 3076,3079
反应条件
1: sec-butylmagnesium chloride With indium(III) chloride in tetrahydrofuran 2: 1-(iodo)-4-methylbenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Heating;
参考文献
Lee, Phil Ho; Lee, Sung Wook; Seomoon, Dong
Organic Letters, 2003 , vol. 5, # 26 p. 4963 - 4966
反应条件
1.1: n-BuLi / tetrahydrofuran / 3 h / 0 - 5 °C 1.2: 10 percent / tetrahydrofuran / 16 h / Heating 2.1: H2 / [Ir-((1Z,5Z)-cyclooct-1,5-diene)][B(3,5-(CF3)2-C6H3)4]; (S)-4-t-Bu-2-(2-(di-o-tolyl-P)phenyl)-4,5-dihydro-oxazole / CH2Cl2 / 1 h / 25 °C / 37503 Torr View Scheme
参考文献
McIntyre, Steven; Hoermann, Esther; Menges, Frederik; Smidt, Sebastian P.; Pfaltz, Andreas
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 2-3 p. 282 - 288
反应条件
anthracene; sodium T=185°C;
参考文献
Pines; Schaap
Journal of the American Chemical Society, 1958 , vol. 80, p. 3076,3079
反应条件
hydrogenchloride T=235°C;
参考文献
Shoesmith; McGechen
Journal of the Chemical Society, 1930 , p. 2231,2234
反应条件
boron trifluoride; phosphorus pentoxide T=70°C;
参考文献
Welsh; Hennion
Journal of the American Chemical Society, 1941 , vol. 63, p. 2603
反应条件
hydrogen fluoride T=0°C;
参考文献
Schlatter; Clark
Journal of the American Chemical Society, 1953 , vol. 75, p. 361,362
反应条件
hydrogen fluoride T=0°C;
参考文献
Schlatter; Clark
Journal of the American Chemical Society, 1953 , vol. 75, p. 361,362
反应条件
sulfuric acid; boron trifluoride
参考文献
Hennion; Kurtz
Journal of the American Chemical Society, 1943 , vol. 65, p. 1001
