T=500°C; P=0.001 - 0.05 Torr; 1 h;

T=700°C; P=0.001 - 0.05 Torr; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

T=500°C; P=0.001 - 0.05 Torr; 1 h;

T=700°C; P=0.001 - 0.05 Torr; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1209227', constants.ctx, '0')">n-butyllithium</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '1730733', constants.ctx, '0')">hexane</a> <br />8&nbsp;h;&nbsp;&nbsp;Yield given;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: SOCl₂ <br />2: BuLi / tetrahydrofuran; hexane / 8 h<br /> <br /> &nbsp;