N'-苄基-N,N-二乙基乙二胺合成路线 （共 8 条）
反应条件
triethylamine in tert-butyl alcohol 12 h; Heating / reflux;
参考文献
HANMI PHARM. CO., LTD.
Patent: WO2007/55514 A1, 2007 ;
Location in patent: Page/Page column 81-82 ;
WO 2007/055514 A1
反应条件
sodium tetrahydroborate; acetic acid; sodium hydroxide in methanol T=20°C;
参考文献
Golchoubian, Hamid; Koohzad, Sara
Transition Metal Chemistry, 2014 , vol. 39, # 3 p. 327 - 335
反应条件
in ethanol T=70°C; 4 h;
参考文献
Watanabe, Toshihiro; Kinoyama, Isao; Kakefuda, Akio; Okazaki, Toshio; Takizawa, Kenji; Hirano, Seiko; Shibata, Hiroshi; Yanagisawa, Isao
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 6 p. 996 - 1007
反应条件
anschliessende Hydrierung an Raney-Nickel;
参考文献
Chapman,N.B.; Taylor,H.
Journal of the Chemical Society, 1961 , p. 1908 - 1918
反应条件
lithium aluminium tetrahydride
参考文献
Rossi,S. et al.
Farmaco, Edizione Scientifica, 1967 , vol. 22, p. 172 - 186
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Chiavarelli; Marini Bettolo
Gazzetta Chimica Italiana, 1951 , vol. 81, p. 89,92
反应条件
sodium; magnesium oxide; decalin
参考文献
I.G.Farbenind.
Patent: DE650491 , 1934 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 24, p. 190
反应条件
hydrogen; palladium 10 on activated carbon in methanol P=760.051 Torr; 48 h;
参考文献
WO2007/55514 A1, ;
Page/Page column 82 ;
WO 2007/055514 A1
参考文献
Searle and Co.
Patent: US2661353 , 1951 ;
