全氟(2-甲基-2-戊烯)合成路线 （共 126 条）
反应条件
potassium carbonate; [3H]-Caproic acid in acetonitrile
3 h;
参考文献
Snegirev, V. F.; Zakharova, E. V.; Makarov, K. N.; Knunyants, I. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 11 p. 2305 - 2312
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 11 p. 2561 - 2568
反应条件
methanol; triethylamine in tetrahydrofuran
T=40°C; 0.5 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Moldavskii; Bispen; Furin; Zhuzhgov
Russian Journal of Applied Chemistry, 1996 , vol. 69, # 4 p. 575 - 582
反应条件
potassium hydroxide; sulfuric acid; phosphorus pentoxide; cesium fluoride
Yield given. Multistep reaction;
参考文献
Bekker, R. A.; Popkova, V. Ya.; Snegirev, V. G.; Knunyants, I. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 3 p. 560 - 564
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 3 p. 621 - 625
反应条件
potassium fluoride in N,N-dimethyl-formamide
T=100°C; 10 h;
参考文献
Ikeda, Isao; Tsuji, Masanori; Okahara, Mitsuo
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 171 - 178
反应条件
1: 90 percent / KOH / -10 °C
2: 83 percent / SO3 / 0.5 h / Heating
3: 74 percent / NaF / 0.58 h / 421 - 436 °C / 0.6 - 1.4 Torr
View Scheme
参考文献
England, David C.
Journal of Organic Chemistry, 1981 , vol. 46, # 1 p. 147 - 153
反应条件
sulfur trioxide; sodium
1) -10 - 0 deg C, methanol, 2) 40 deg C; Yield given. Multistep reaction;
参考文献
England, David C.
Journal of Organic Chemistry, 1981 , vol. 46, # 1 p. 147 - 153
