顺-八氢-2-(1H)萘酮合成路线 (共 61 条)
反应条件
oxygen; Co-Ce-NH4Br T=110°C; P=760 Torr; 0.5 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yazu, Kaumasa; Wakabayashi, Takeshige; Nakayama, Tetsuo
Chemistry Letters, 1986 , p. 1409 - 1412
反应条件
oxygen; Co-Ce-NH4Br T=100°C; P=760 Torr; 0.5 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yazu, Kaumasa; Wakabayashi, Takeshige; Nakayama, Tetsuo
Chemistry Letters, 1986 , p. 1409 - 1412
反应条件
hydrogen; palladium on activated charcoal in tert-butyl alcohol T=80°C; P=30002.4 - 37503 Torr; oth. catalysts; Product distributionRate constant;
参考文献
Nishimura; Ohbuchi; Ikeno; Okada
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 9 p. 2557 - 2564
反应条件
1: n-BuLi 2: 77 percent / HgCl2, H2O / acetonitrile / 24 h / Heating 3: hydrogen / 10percent Pd/C View Scheme
参考文献
Jones, J. Bryan; Dodds, David R.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 2397 - 2404
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran; water
参考文献
Yonehara, Fumi; Kido, Yoshiyuki; Sugimoto, Hiraku; Morita, Satoshi; Yamaguchi, Masahiko
Journal of Organic Chemistry, 2003 , vol. 68, # 17 p. 6752 - 6759
反应条件
perchloric acid; dihydrogen peroxide in water; acetonitrile; tert-butyl alcohol T=59.84°C; 1 h; regioselective reaction;
参考文献
Kamata, Keigo; Yonehara, Kazuhiro; Nakagawa, Yoshinao; Uehara, Kazuhiro; Mizuno, Noritaka
Nature Chemistry, 2010 , vol. 2, # 6 p. 478 - 483
反应条件
lithium aluminium tetrahydride; titanium tetrachloride 1) THF, -78 deg C, HMPA; 2) THF; 3) CH2Cl2; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Macdonald, Timothy L.; Mahalingam, Sankaran
Journal of the American Chemical Society, 1980 , vol. 102, # 6 p. 2113 - 2115
反应条件
(tBuOOCO)2; decatungstate in acetonitrile T=60°C; 2 h; Irradiationvar. polyoxometalates; Product distributionMechanism;
参考文献
Combs-Walker, Lucille A.; Hill, Craig L.
Journal of the American Chemical Society, 1992 , vol. 114, # 3 p. 938 - 946
反应条件
Fe(triflate)2(1-(6-methyl-2-pyridylmethyl)-4,7-dimethyl-1,4,7-triazacyclononane); dihydrogen peroxide; acetic acid in water; acetonitrile T=0°C; 0.666667 h; Reagent/catalyst;
参考文献
Prat, Irene; Gomez, Laura; Canta, Merce; Ribas, Xavi; Costas, Miquel
Chemistry - A European Journal, 2013 , vol. 19, # 6 p. 1908 - 1913
反应条件
potassium dichromate; sulfuric acid T=30°C;
参考文献
Nikitin
Zhurnal Obshchei Khimii, 1945 , vol. 15, p. 401,403
Chem.Abstr., 1946 , p. 4706