顺-八氢-2-(1H)萘酮合成路线 (共 61 条)
反应条件
((C4H9)4)4W10O32 in acetonitrile T=25°C; Irradiation;
参考文献
Combs-Walker, Lucille A.; Hill, Craig L.
Journal of the American Chemical Society, 1992 , vol. 114, # 3 p. 938 - 946
反应条件
methyl(trifluoromethyl)dioxirane in dichloromethane T=-22°C; 0.183333 h;
参考文献
Mello, Rossella; Fiorentino, Michele; Fusco, Caterina; Curci, Ruggero
Journal of the American Chemical Society, 1989 , vol. 111, # 17 p. 6749 - 6757
反应条件
1: With ammonia; lithium; tert-butyl alcohol in tetrahydrofuran T=-70°C; 0.25 h; 2: With Jone's reagent in acetone T=0°C; 0.25 h;
参考文献
Kaneko, Yuki; Kiyotsuka, Yohei; Acharya, Hukum P.; Kobayashi, Yuichi
Chemical Communications, 2010 , vol. 46, # 30 p. 5482 - 5484
反应条件
palladium Hydrogenation;
参考文献
Chikashita, Hidenori; Miyazaki, Makoto; Itoh, Kazuyoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 699 - 706
反应条件
1: H2 / Pd-C / methanol 2: benzene; methanol / Irradiation 3: H2 / Pd-C / methanol View Scheme
参考文献
Takakis,J.M.; Agosta,W.C.
Journal of the American Chemical Society, 1979 , vol. 101, # 9 p. 2383 - 2389
反应条件
oxygen; Co-Ce-NH4Br in acetic anhydride T=90°C; P=760 Torr; 2 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yazu, Kaumasa; Wakabayashi, Takeshige; Nakayama, Tetsuo
Chemistry Letters, 1986 , p. 1409 - 1412
反应条件
oxygen; Co-Ce-NH4Br in acetic anhydride T=95°C; P=760 Torr; 1 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yazu, Kaumasa; Wakabayashi, Takeshige; Nakayama, Tetsuo
Chemistry Letters, 1986 , p. 1409 - 1412
反应条件
oxygen; Co-Ce-NH4Br in acetic anhydride T=100°C; P=760 Torr; 0.5 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yazu, Kaumasa; Wakabayashi, Takeshige; Nakayama, Tetsuo
Chemistry Letters, 1986 , p. 1409 - 1412
反应条件
potassium dichromate; sulfuric acid in diethyl ether Oxidation; 6 h;
参考文献
Chatterjee, Asima; Sahu, Arabinda; Saha, Munmun; Banerji, Julie
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1997 , vol. 36, # 2 p. 121 - 122
反应条件
ammonia; lithium; tert-butyl alcohol in tetrahydrofuran T=-70°C; 0.25 h;
参考文献
Kaneko, Yuki; Kiyotsuka, Yohei; Acharya, Hukum P.; Kobayashi, Yuichi
Chemical Communications, 2010 , vol. 46, # 30 p. 5482 - 5484