2-氯-2,3-二氢-1H-茚-1-酮合成路线 （共 13 条）
反应条件
iodobenzene dichloride in methanol T=20°C;
参考文献
Yu, Jun; Zhang, Chi
Synthesis, 2009 , # 14 art. no. F02709SS, p. 2324 - 2328
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; trifluoromethane sulfonylchloride in benzene T=120°C; 7 h;
参考文献
Kamigata, Nobumasa; Udodaira, Kumiko; Shimizu, Toshio
Phosphorus, Sulfur and Silicon and Related Elements, 1997 , vol. 129, p. 155 - 168
反应条件
1: With aluminium trichloride in dichloromethane T=20°C; 0.166667 h; 2: With 2,4,5-trichloropyridazin-3(2H)-one in dichloromethane T=20°C; 2 h;
参考文献
Moon, Byung Seok; Choi, Han Young; Koh, Hun Yeong; Chi, Dae Yoon
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 2 p. 472 - 476
反应条件
iodobenzene dichloride T=20°C; 0.5 h; Molecular sieve;
参考文献
Yu, Jun; Zhang, Chi
Synthesis, 2009 , # 14 art. no. F02709SS, p. 2324 - 2328
反应条件
Catalyst M-Chromium oxide; sulfuric acid
参考文献
Courtot; Fayet; Parant
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1928 , vol. 186, p. 372
反应条件
in cyclohexane 15 h; Irradiation; Product distributionMechanism;
参考文献
Sket, Boris; Zupan, Marko
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 8 p. 1745 - 1752
参考文献
Courtot; Fayet; Parant
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1928 , vol. 186, p. 372
参考文献
Goldschmidt; Endres; Dirsch
Chemische Berichte, 1925 , vol. 58, p. 574
反应条件
potassium hydroxide; methyllithium in tetrahydrofuran; methanol; diethyl ether; pentane
参考文献
University of Bath; University of Cincinnati
Patent: US5185360 A1, 1993 ;
反应条件
methyllithium; tert.-butyl lithium 1) THF, pentane, -78 deg C, 1 h, 2) a) THF, -78 deg C, 2h, b) to room temp., overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Graham, Jeremy; Ninan, Aleyamma; Reza, Khalid; Sainsbury, Malcolm; Shertzer, Howard G.
Tetrahedron, 1992 , vol. 48, # 1 p. 167 - 176
