N-叔丁氧羰基-L-丙氨酸合成路线 (共 171 条)
反应条件
1: With methanol; copper(II) bis(trifluoromethanesulfonate) T=20°C; 16 h; 2: With Ba(OH)2 in methanol; water T=20°C; 3: With citric acid in methanol; water pH=4 - 5;
参考文献
Broehmer, Manuel C.; Mundinger, Stephan; Braese, Stefan; Bannwarth, Willi
Angewandte Chemie - International Edition, 2011 , vol. 50, # 27 p. 6175 - 6177
反应条件
4-(N,N-dimethlyamino)pyridine in 1,4-dioxane; water Ambient temperature;
参考文献
Kunieda, Takehisa; Higuchi, Tsunehiko; Abe, Yoshihiro; Hirobe, Masaaki
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 6 p. 2174 - 2181
反应条件
ruthenium trichloride; sodium periodate; sodium carbonate in tetrachloromethane; water; acetonitrile
参考文献
Poch, Marta
Tetrahedron Letters, 1993 , vol. 34, # 48 p. 7781 - 7784
反应条件
1: 1.) sodium bis(trimethylsilyl)amide / 1.) THF, -82 deg C, 35 min, 2.) THF, -82 deg C, 1.5 h 2: 54 percent / Li, NH3(liquid), ethanol / tetrahydrofuran / 1 h / -33 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 113, # 24 p. 9276 - 9286
反应条件
triethylamine in 1,4-dioxane Ambient temperature;
参考文献
Phillips, Lawrence R.; Nishimura, Osamu; Fraser, Blair A.
Carbohydrate Research, 1984 , vol. 132, p. 275 - 286
反应条件
tertiary amine in 1,4-dioxane; water 3 h;
参考文献
Henklein, Peter; Heyne, Hans-Ulrich; Halatsch, Wolf-Rainer; Niedrich, Hartmut
Synthesis, 1987 , # 2 p. 166 - 167
反应条件
potassium carbonate in water; N,N-dimethyl-formamide 0.5 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 44, # 16 p. 5101 - 5108
反应条件
1: 80 percent / Et3N / acetonitrile / 5 h / 5 °C 2: 82 percent / Et3N / H2O / Ambient temperature View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 10 p. 3103 - 3108
反应条件
helical substituted polyacetylene-(R)-camphor-10-sulfonamide in chloroform T=25 - 35°C; enantioselective reaction;
参考文献
Macromolecules, , vol. 44, # 18 p. 7109 - 7114
反应条件
triethylamine in water; acetonitrile 24 h; Ambient temperature;
参考文献
Ohta, Akihiro; Inagawa, Yukiko; Inoue, Masami; Shimazaki, Makoto; Mamiya, Yukari
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1173 - 1177