1,4-二乙酰氧基-2-丁烯合成路线 （共 39 条）
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene 5 h; Ambient temperature;
参考文献
Crilley, Martine M. L.; Golding, Bernard T.; Pierpoint, Colin
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2061 - 2068
反应条件
Ru(C6H2(CH3)3NC3H4NC10H14)(OOCC(CH3)3)(CHC6H4OCH(CH3)2) in THF-d8 (tetrahydrofuran-d8) T=35°C; 4 h; Sealed flaskInert atmosphere;
参考文献
Occhipinti, Giovanni; Hansen, Fredrik R.; Toernroos, Karl W.; Jensen, Vidar R.
Journal of the American Chemical Society, 2013 , vol. 135, # 9 p. 3331 - 3334
反应条件
bis(tricyclohexylphosphine)benzylidene ruthenium(IV) dichloride in benzene 1.5 h; Ambient temperature;
参考文献
Michaut, Mathieu; Parrain, Jean-Luc; Santelli, Maurice
Chemical Communications, 1998 , # 23 p. 2567 - 2568
反应条件
in acetic acid 24 h; Heating;
参考文献
Bouquillon, Sandrine; Muzart, Jacques
European Journal of Organic Chemistry, 2001 , # 17 p. 3301 - 3305
反应条件
tetrakis(triphenylphosphine) palladium(0) in dichloromethane T=20°C; 48 h;
参考文献
Chavez, Cesar Sandoval; Rudler, Henri; Parlier, Andree; Herson, Patrick
Tetrahedron Letters, 2008 , vol. 49, # 41 p. 5843 - 5846
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=70 - 72°C; Product distribution;
参考文献
Mitsubishi Chemical Corporation
Patent: US6300515 B1, 2001 ;
反应条件
sodium acetate in acetic anhydride; acetic acid T=60°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Uemura, Sakae; Miyoshi, Haruo; Tabata, Akira; Okano, Masaya
Tetrahedron, 1981 , vol. 37, p. 291 - 295
反应条件
potassium acetate in acetic acid
参考文献
Heasley,V.L.; Chamberlain,P.H.
Journal of Organic Chemistry, 1970 , vol. 35, p. 539 - 541
反应条件
potassium carbonate 1.5 h; Reflux;
参考文献
Mallesha; Rao, S. Prahlada; Suhas; Gowda, D. Channe
Journal of Chemical Research, 2011 , vol. 35, # 9 p. 536 - 539
反应条件
C45H64Cl2N3PRu in dichloromethane-d2 T=20 - 45°C; Inert atmosphere;
参考文献
Storvick, Jennifer M.; Ankoudinova, Evgenia; King, Brianne R.; Van Epps, Heather; O'Neil, Gregory W.
Tetrahedron Letters, 2011 , vol. 52, # 44 p. 5858 - 5861
