N-苄基-对甲苯磺酸胺合成路线 (共 161 条)
反应条件
1.1: 70 percent / NEt3 / CH2Cl2 / 2 h / 20 °C 2.1: tetrahydrofuran / -78 - 0 °C 2.2: 95 percent / H2O / tetrahydrofuran View Scheme
参考文献
Chemical Communications, , # 7 p. 933 - 935
反应条件
1.1: 60 percent / K2CO3 / acetonitrile / 24 h / Heating 2.1: 70 percent / NEt3 / CH2Cl2 / 2 h / 20 °C 3.1: tetrahydrofuran / -78 - 0 °C 3.2: 95 percent / H2O / tetrahydrofuran View Scheme
参考文献
Chemical Communications, , # 7 p. 933 - 935
反应条件
1: n-butyllithium / tetrahydrofuran 2: 85 percent / tetraethylammonium p-toluenesulfonate / methanol / Electrochemical reaction; reticulated vitreous carbon anode; Pt cathode View Scheme
参考文献
Organic Letters, , vol. 4, # 10 p. 1763 - 1766
反应条件
1: 85 percent / thionyl chloride 2: n-butyllithium / tetrahydrofuran 3: 85 percent / tetraethylammonium p-toluenesulfonate / methanol / Electrochemical reaction; reticulated vitreous carbon anode; Pt cathode View Scheme
参考文献
Organic Letters, , vol. 4, # 10 p. 1763 - 1766
反应条件
[(Cp*Ir)2(μ-NTs)2]; potassium tert-butylate in toluene 17 h; Inert atmosphereReflux;
参考文献
Organic Letters, , vol. 12, # 6 p. 1336 - 1339
反应条件
TMS-SnBu3; cesium fluoride in N,N-dimethyl-formamide T=100°C; P=7500.75 Torr; 3 h; Autoclave;
参考文献
Chemistry - A European Journal, , vol. 19, # 3 p. 1123 - 1128
反应条件
Co(acacen) T=75°C; 3 h;
参考文献
Journal of Organometallic Chemistry, , vol. 690, # 8 SPEC. ISS. p. 2142 - 2148
反应条件
1: carbon dioxide; benzaldehyde; toluene-4-sulfonamide With TMS-SnBu3; cesium fluoride in N,N-dimethyl-formamide T=100°C; P=7500.75 Torr; 3 h; Autoclave; 2: diazomethyl-trimethyl-silane in methanol; diethyl ether
参考文献
Chemistry - A European Journal, , vol. 19, # 3 p. 1123 - 1128
反应条件
sodium hydroxide in ethanol
参考文献
Journal of Organic Chemistry, , vol. 36, p. 4102 - 4105
反应条件
in acetonitrile Heating;
参考文献
Bieraeugel, H.; Plemp, R.; Hiemstra, H. C.; Pandit, U. K.
Tetrahedron, 1983 , vol. 39, # 23 p. 3971 - 3980