N-苄基-对甲苯磺酸胺合成路线 （共 161 条）
反应条件
1: methanol / 4.5 h / 20 °C / Reflux 2: titanium tetrachloride / tetrachloroethane, 1,1,2,2- / 48 h / 120 °C / sealed tube View Scheme
参考文献
Synlett, , # 4 p. 595 - 600
反应条件
1: bromine / water 2: potassium carbonate / 5 h / 80 °C / Inert atmosphere View Scheme
参考文献
Chemical Communications, , vol. 48, # 44 p. 5491 - 5493
反应条件
2: Raney-Ni / ethanol / 1.5 h / 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 43, # 2 p. 198 - 207,10
反应条件
1: carbon dioxide; toluene-4-sulfonamide; ((trimethylsilyl)oxy)(phenyl(CH))tributylstannane With 1,1,1,2,2,2-hexabutyl-distannane; cesium fluoride P=7500.75 Torr; 2: diazomethyl-trimethyl-silane in methanol; diethyl ether
参考文献
Chemistry - A European Journal, , vol. 19, # 3 p. 1123 - 1128
反应条件
1: carbon dioxide; N-tosyl-α-(tributylstannyl)benzylamine; toluene-4-sulfonamide With 1,1,1,2,2,2-hexabutyl-distannane; cesium fluoride P=7500.75 Torr; 2: diazomethyl-trimethyl-silane in methanol; diethyl ether
参考文献
Chemistry - A European Journal, , vol. 19, # 3 p. 1123 - 1128
反应条件
1: sodium tetrahydroborate; sodium hydroxide / methanol / 18 - 25 °C / |Cooling; |Inert atmosphere 2: [Cp*Ir(SnCl3)2{SnCl2(H2O)2}] / 1,2-dichloro-ethane / 70 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Tetrahedron, , vol. 69, # 2 p. 942 - 956
反应条件
tetraethylammonium cyanide in dimethylsulfoxide-d6 T=20°C; KineticsProduct distribution; Further Variations:ReagentsSolventsTemperatures;
参考文献
Journal of Organic Chemistry, , vol. 66, # 17 p. 5679 - 5686
反应条件
1: carbon dioxide; 4-(methoxy)benzenesulfonamide; N-tosyl-α-(tributylstannyl)benzylamine With 1,1,1,2,2,2-hexabutyl-distannane; cesium fluoride P=7500.75 Torr; 2: diazomethyl-trimethyl-silane in methanol; diethyl ether
参考文献
Chemistry - A European Journal, , vol. 19, # 3 p. 1123 - 1128
反应条件
1: 91 percent / CH2Cl2 / 13 h / Heating 2: 70 percent / acetonitrile / Heating View Scheme
参考文献
Tetrahedron, , vol. 39, # 23 p. 3971 - 3980
反应条件
pyridine; Rink amide resin; potassium tert-butylate; trifluoroacetic acid 1.) CH2Cl2, room temp., 15 h, 2.) THF, 50 deg C, 2 h, 3.) CH2Cl2, 15 min; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 37, # 8 p. 1145 - 1148
