N-苄基-对甲苯磺酸胺合成路线 (共 161 条)
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane T=0 - 20°C; 16 h;
参考文献
Heffernan, Stephen J.; Beddoes, James M.; Mahon, Mary F.; Hennessy, Alan J.; Carbery, David R.
Chemical Communications, 2013 , vol. 49, # 23 p. 2314 - 2316
反应条件
palladium diacetate; potassium carbonate in toluene T=150°C; 8 h;
参考文献
Feng, Sun Lin; Liu, Chuan Zhi; Li, Qiang; Yu, Xiao Chun; Xu, Qing
Chinese Chemical Letters, 2011 , vol. 22, # 9 p. 1021 - 1024
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 1.5 h;
参考文献
Palakurthy, Nani Babu; Mandal, Bhubaneswar
Tetrahedron Letters, 2011 , vol. 52, # 52 p. 7132 - 7134
反应条件
titanium tetrachloride in tetrachloroethane, 1,1,2,2- T=120°C; 48 h; sealed tube;
参考文献
Chen, Jiayan; Dang, Ling; Li, Qiang; Ye, Yong; Fu, Shaomin; Zeng, Wei
Synlett, 2012 , # 4 p. 595 - 600
反应条件
formic acid; C6H15N*C31H37ClN2O2RhS*ClH; triethylamine in ethyl acetate Inert atmosphere;
参考文献
Kwak, Se Hun; Lee, Sun Ah; Lee, Kee-In
Tetrahedron Asymmetry, 2010 , vol. 21, # 7 p. 800 - 804
反应条件
1: 2-monochloropropane With zinc(II) chloride in tetrahydrofuran T=20°C; 1 h; 2: [N(E)]-4-methyl-N-(phenylmethylene)benzenesulfonamide in tetrahydrofuran T=20°C; 2 h;
参考文献
Journal of the American Chemical Society, , vol. 128, # 31 p. 9998 - 9999
反应条件
1: ethyl magnesium chloride With zinc(II) chloride in tetrahydrofuran T=20°C; 1 h; 2: [N(E)]-4-methyl-N-(phenylmethylene)benzenesulfonamide in tetrahydrofuran T=20°C; 2 h;
参考文献
Journal of the American Chemical Society, , vol. 128, # 31 p. 9998 - 9999
反应条件
hydrogen; palladium dihydroxide in ethanol P=760.051 Torr;
参考文献
Johnson II, David C.; Widlanski, Theodore S.
Tetrahedron Letters, 2004 , vol. 45, # 46 p. 8483 - 8487
反应条件
4 A molecular sieve; [Cu(I)(CH3CN)4]PF6 in acetonitrile T=65 - 70°C; 10 h;
参考文献
Bhuyan, Ranjana; Nicholas, Kenneth M.
Organic Letters, 2007 , vol. 9, # 20 p. 3957 - 3959
反应条件
1: bis-lt;(4-methylphenyl)methylgt;disulfide With tert-butylhypochlorite; water in acetonitrile T=0°C; 0.25 h; 2: benzylamine in acetonitrile T=0 - 20°C; 0.666667 h;
参考文献
Joyard, Yoann; Papamicael, Cyril; Bohn, Pierre; Bischoff, Laurent
Organic Letters, 2013 , vol. 15, # 9 p. 2294 - 2297