1: acetic anhydride, p-TsOH / toluene / 1 h / Heating 2: m-chloroperbenzoic acid / CH2Cl2 / 1 h / 0 °C 3: 48 percent / pyridine / 3 h / Heating View Scheme
参考文献
Watanabe, Mikio; Nakamori, Seijin; Hasegawa, Hatsue; Shirai, Kozo; Kumamoto, Takanobu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 3 p. 817 - 821
1: aq. NaOH / ethanol / 6 h / Heating 2: H2SO4 / ethanol / 10 h / Heating 3: sodium metaperiodate / H2O; ethanol / 12 h / 0 °C 4: acetic anhydride, p-TsOH / toluene / 1 h / Heating 5: m-chloroperbenzoic acid / CH2Cl2 / 1 h / 0 °C 6: 48 percent / pyridine / 3 h / Heating View Scheme
参考文献
Watanabe, Mikio; Nakamori, Seijin; Hasegawa, Hatsue; Shirai, Kozo; Kumamoto, Takanobu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 3 p. 817 - 821
ethyl bromoacetate; zinc; benzene Erhitzen des Reaktionsprodukts mit Bromwasserstoff in Essigsaeure;
参考文献
Kariyone; Fukui
Yakugaku Zasshi, 1946 , vol. 66, p. 42
Chem.Abstr., 1951 , p. 6605
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Linville; Elderfield
Journal of Organic Chemistry, 1941 , vol. 6, p. 270
