Watanabe, Mikio; Nakamori, Seijin; Hasegawa, Hatsue; Shirai, Kozo; Kumamoto, Takanobu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 3 p. 817 - 821
1: 100 percent / sodium borohydride / methanol / 3 h / 0 °C 2: phosphorus tribromide / CCl4 / Heating 3: ethanol / 4 h / Heating 4: aq. NaOH / ethanol / 6 h / Heating 5: H2SO4 / ethanol / 10 h / Heating 6: sodium metaperiodate / H2O; ethanol / 12 h / 0 °C 7: acetic anhydride, p-TsOH / toluene / 1 h / Heating 8: m-chloroperbenzoic acid / CH2Cl2 / 1 h / 0 °C 9: 48 percent / pyridine / 3 h / Heating View Scheme
参考文献
Watanabe, Mikio; Nakamori, Seijin; Hasegawa, Hatsue; Shirai, Kozo; Kumamoto, Takanobu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 3 p. 817 - 821
1: phosphorus tribromide / CCl4 / Heating 2: ethanol / 4 h / Heating 3: aq. NaOH / ethanol / 6 h / Heating 4: H2SO4 / ethanol / 10 h / Heating 5: sodium metaperiodate / H2O; ethanol / 12 h / 0 °C 6: acetic anhydride, p-TsOH / toluene / 1 h / Heating 7: m-chloroperbenzoic acid / CH2Cl2 / 1 h / 0 °C 8: 48 percent / pyridine / 3 h / Heating View Scheme
参考文献
Watanabe, Mikio; Nakamori, Seijin; Hasegawa, Hatsue; Shirai, Kozo; Kumamoto, Takanobu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 3 p. 817 - 821
1: ethanol / 4 h / Heating 2: aq. NaOH / ethanol / 6 h / Heating 3: H2SO4 / ethanol / 10 h / Heating 4: sodium metaperiodate / H2O; ethanol / 12 h / 0 °C 5: acetic anhydride, p-TsOH / toluene / 1 h / Heating 6: m-chloroperbenzoic acid / CH2Cl2 / 1 h / 0 °C 7: 48 percent / pyridine / 3 h / Heating View Scheme
参考文献
Watanabe, Mikio; Nakamori, Seijin; Hasegawa, Hatsue; Shirai, Kozo; Kumamoto, Takanobu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 3 p. 817 - 821
1: m-chloroperbenzoic acid / CH2Cl2 / 1 h / 0 °C 2: 48 percent / pyridine / 3 h / Heating View Scheme
参考文献
Watanabe, Mikio; Nakamori, Seijin; Hasegawa, Hatsue; Shirai, Kozo; Kumamoto, Takanobu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 3 p. 817 - 821
1: sodium metaperiodate / H2O; ethanol / 12 h / 0 °C 2: acetic anhydride, p-TsOH / toluene / 1 h / Heating 3: m-chloroperbenzoic acid / CH2Cl2 / 1 h / 0 °C 4: 48 percent / pyridine / 3 h / Heating View Scheme
参考文献
Watanabe, Mikio; Nakamori, Seijin; Hasegawa, Hatsue; Shirai, Kozo; Kumamoto, Takanobu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 3 p. 817 - 821
