1,4-二乙酰氧基-2-丁炔合成路线 （共 37 条）
反应条件
sodium hydroxide in dichloromethane 1.) r.t., overnight. 2.) reflux, 2 h;
参考文献
Malanga, Corrado; Mannucci, Serena; Lardicci, Luciano
Tetrahedron, 1998 , vol. 54, # 7 p. 1021 - 1028
反应条件
titanium tetrachloride in dichloromethane T=0 - 25°C; Acetylation; 6 h;
参考文献
Chandrasekhar; Ramachandar; Reddy, M. Venkat; Takhi, Mohamed
Journal of Organic Chemistry, 2000 , vol. 65, # 15 p. 4729 - 4731
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane); tri-n-butyl-tin hydride in tetrahydrofuran 0.5 h; Ambient temperature;
参考文献
Malanga, Corrado; Mannucci, Serena; Lardicci, Luciano
Tetrahedron, 1998 , vol. 54, # 7 p. 1021 - 1028
反应条件
lithium bis(perfluorooctylsulfonyl)amide T=30°C; 42 h; Catalytic behavior; Reagent/catalystTime;
参考文献
Li, Guilong; Zhao, Gang
Synthetic Communications, 2013 , vol. 43, # 1 p. 34 - 43,10
反应条件
sodium hydrogen sulphate; silica gel in hexane T=50°C; 7 h;
参考文献
Journal of Organic Chemistry, , vol. 57, # 1 p. 312 - 316
反应条件
pyridine in dichloromethane
参考文献
Troyanskii, E. I.; Strelenko, Yu. A.; Demchuk, D. V.; Samoshin, V. V.; Lutsenko, A. I.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 8.2 p. 1629 - 1636
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 8 p. 1841 - 1849
反应条件
di-isopropyl ether; toluene-4-sulfonic acid 12 h;
参考文献
Werner, Wolfgang
Journal of Chemical Research, Miniprint, 1980 , # 6 p. 2769 - 2775
反应条件
potassium carbonate 1 h; Reflux;
参考文献
Mallesha; Rao, S. Prahlada; Suhas; Gowda, D. Channe
Journal of Chemical Research, 2011 , vol. 35, # 9 p. 536 - 539
反应条件
sodium hydride in tetrahydrofuran
参考文献
Journal of Organic Chemistry, , vol. 57, # 1 p. 312 - 316
反应条件
in pyridine; hexane T=80°C; 1 h; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, p. 838 - 841
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 4 p. 911 - 913
