2-(2-呋喃基)-苯并噻唑合成路线 (共 31 条)
反应条件
trichlorophosphate T=100°C; Vilsmeier-Haack formylation; 2 h;
参考文献
Paizs, Csaba; Tosa, Monica; Majdik, Cornelia; Taehtinen, Petri; Irimie, Florin Dan; Kanerva, Liisa T.
Tetrahedron Asymmetry, 2003 , vol. 14, # 5 p. 619 - 627
反应条件
PPA T=80 - 90°C; 3 h;
参考文献
Melnikova; Elchaninov; Milov; Lukyanov
Chemistry of Heterocyclic Compounds, 2008 , vol. 44, # 9 p. 1070 - 1076
反应条件
tert.-butylhydroperoxide; copper dichloride in water
T=80°C; 24.5 h; Inert atmosphereSchlenk technique;
参考文献
Zhang, Mingliang; Lu, Wen-Ting; Ruan, Wenqing; Zhang, Hui-Jun; Wen, Ting-Bin
Tetrahedron Letters, 2014 , vol. 55, # 10 p. 1806 - 1809
反应条件
Iron (III) nitrate nonahydrate; dihydrogen peroxide
T=50°C; 0.1 h;
参考文献
Bahrami, Kiumars; Khodaei, Mohammad Mehdi; Naali, Fardin
Synlett, 2009 , # 4 p. 569 - 572
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 1,10-phenanthroline; copper (II) acetate monohydrate; sulfur in dimethyl sulfoxide
T=100°C;
参考文献
Wang, Rui; Ding, Yong-Liang; Liu, Hong; Peng, Shu; Ren, Jie; Li, Lei
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 945 - 949
反应条件
in neat (no solvent)
1 h; Green chemistry; Time;
参考文献
Yoon, Soon Byung; Chun, Eun Jeong; Noh, Young Ri; Yoon, Yong Jin; Lee, Sang-Geyong
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 9 p. 2819 - 2821
反应条件
copper(I) bromide dimethylsulfide complex; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether
Stille cross-coupling; 3 h; Heating;
参考文献
Alphonse, France-Aimee; Suzenet, Franck; Keromnes, Anne; Lebret, Bruno; Guillaumet, Gerald
Organic Letters, 2003 , vol. 5, # 6 p. 803 - 805
反应条件
tetrakis(triphenylphosphine) palladium(0); Cu(I) 3-methylsalicylate in tetrahydrofuran
T=50°C; 14 h;
参考文献
Egi, Masahiro; Liebeskind, Lanny S
Organic letters, 2003 , vol. 5, # 6 p. 801 - 802
反应条件
copper diacetate; triethylamine in ethanol
T=70°C; 6 h;
参考文献
Sun, Yadong; Jiang, Huanfeng; Wu, Wanqing; Zeng, Wei; Wu, Xia
Organic Letters, 2013 , vol. 15, # 7 p. 1598 - 1601
反应条件
toluene-4-sulfonic acid in PEG-200/400
0.166667 h; Microwave irradiation;
参考文献
Deligeorgiev, Todor G.; Kaloyanova, Stefka; Vasilev, Aleksey; Vaquero, Juan J.
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 11 p. 2292 - 2302