tert-butylamine in tetrahydrofuran stannane added to chloride, 10 molar equiv. of additive, stirred under nitrogen at 0°C 3 h; quenched with aq. ammonium chloride;
lithium aluminium tetrahydride in tetrahydrofuran 48 h; Ambient temperaturein the dark; the other compound was the unreacted starting material in the reaction mixture; MechanismProduct distribution;
参考文献
Ashby, E. C.; DePriest, R. N.; Pham, T. N.
Tetrahedron Letters, 1983 , vol. 24, # 28 p. 2825 - 2828
