反应条件
1.1: 86 percent / boron tribromide / CH2Cl2 / -78 - 20 °C
2.1: 93 percent / CH2Cl2
3.1: 87 percent / triphenylphosphine; coppe(I) iodide / bis(triphenylphosphine)palladium(II) chloride / triethylamine / 20 h / 80 °C
4.1: methanol / Heating
4.2: 95 percent / potassium carbonate / methanol / 20 °C
View Scheme
参考文献
Kastler, Marcel; Schmidt, Jochen; Pisula, Wojciech; Sebastiani, Daniel; Muellen, Klaus
Journal of the American Chemical Society, 2006 , vol. 128, # 29 p. 9526 - 9534
