5-(甲氧基甲烯基)-2,2-二甲基-1,3-二氧己环-4,6-二酮合成路线 （共 30 条）
参考文献
Jourdain; Pommelet
Synthetic Communications, 1997 , vol. 27, # 3 p. 483 - 492
参考文献
Morgentin, Remy; Pasquet, Georges; Boutron, Pascal; Jung, Frederic; Lamorlette, Maryannick; Maudet, Mickael; Ple, Patrick
Tetrahedron, 2008 , vol. 64, # 12 p. 2772 - 2782
反应条件
in acetonitrile 0.166667 h; Ambient temperature;
参考文献
Blake, Alexander J.; Hunter, Gordon A.; McNab, Hamish
Journal of Chemical Research, Miniprint, 1989 , # 5 p. 921 - 943
参考文献
S P A SOCIETA' PRODOTTI ANTIBIOTICI S.p.a.
Patent: EP310849 A1, 1989 ;
反应条件
ytterbium(III) triflate in nitromethane T=100°C; 1.5 h;
参考文献
Fillion, Eric; Dumas, Aaron M.; Kuropatwa, Bryan A.; Malhotra, Neil R.; Sitler, Tamsyn C.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 409 - 412
反应条件
ytterbium(III) triflate in nitromethane T=100°C; 1.5 h;
参考文献
Fillion, Eric; Dumas, Aaron M.; Kuropatwa, Bryan A.; Malhotra, Neil R.; Sitler, Tamsyn C.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 409 - 412
反应条件
ytterbium(III) triflate in 1,2-dichloro-ethane T=100°C; 1.5 h;
参考文献
Fillion, Eric; Dumas, Aaron M.; Kuropatwa, Bryan A.; Malhotra, Neil R.; Sitler, Tamsyn C.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 409 - 412
反应条件
trifluorormethanesulfonic acid in 1,2-dichloro-ethane T=100°C; 1.5 h;
参考文献
Fillion, Eric; Dumas, Aaron M.; Kuropatwa, Bryan A.; Malhotra, Neil R.; Sitler, Tamsyn C.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 409 - 412
反应条件
in acetonitrile T=20°C; 0.25 h;
参考文献
Hill, Lawrence; Imam, S. Haider; McNab, Hamish; O'Neill, William J.
Synlett, 2009 , # 11 p. 1847 - 1851
反应条件
trimethyl orthoformate T=50°C; 2 h; Reflux;
参考文献
Wang, Min; Gao, Mingzhang; Miller, Kathy D.; Sledge, George W.; Zheng, Qi-Huang
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 4 p. 1569 - 1574
