1-(异丙基硫基)-2-甲基苯合成路线 （共 10 条）
反应条件
(i) NaOEt, EtOH, (ii) /BRN= 1098244/; Multistep reaction;
参考文献
Bourrain, Sylvie; Hunt, Peter Alan; Huscroft, Ian Thomas; Kulagowski, Janusz Jozef; London, Clare; Naylor, Elizabeth Mary; Raubo, Piotr Antoni; Seward, Eileen Mary
Patent: US2004/229864 A1, 2004 ;
Location in patent: Page/Page column 6 ;
US 20040229864 A1
反应条件
NiCl2((PPh3)P)2 in benzene T=25°C; 2 h;
参考文献
Tiecco, Marcello; Testaferri, Lorenzo; Tingoli, Marco; Chianelli, Donatella; Wenkert, Ernest
Tetrahedron Letters, 1982 , vol. 23, # 44 p. 4629 - 4632
反应条件
NiCl2((PPh3)P)2 in diethyl ether; benzene T=50°C;
参考文献
Tiecco, M.; Testaferri, L.; Tingoli, M.; Wenkert, E.
Tetrahedron, 1983 , vol. 39, # 13 p. 2289 - 2294
反应条件
NiCl2((PPh3)P)2 in diethyl ether; benzene 2.5 h; Ambient temperature;
参考文献
Tingoli, Marco; Tiecco, Marcello; Testaferri, Lorenzo; Chianelli, Donatella
Gazzetta Chimica Italiana, 1991 , vol. 121, # 2 p. 59 - 61
反应条件
2: 63 percent / Ni(PPh3)2Cl2 / benzene / 2 h / 25 °C View Scheme
参考文献
Tiecco, Marcello; Testaferri, Lorenzo; Tingoli, Marco; Chianelli, Donatella; Wenkert, Ernest
Tetrahedron Letters, 1982 , vol. 23, # 44 p. 4629 - 4632
反应条件
n-butyllithium; potassium tert-butylate 1.) hexane, from -20 deg C to -10 deg C, 4 h, 2.) hexane, RT, overnight; Yield given. Multistep reaction;
参考文献
Cabiddu, S.; Fattuoni, C.; Floris, C.; Gelli, G.; Melis, S.
Journal of Organometallic Chemistry, 1992 , vol. 441, # 2 p. 197 - 202
参考文献
Gasparic et al.
Collection of Czechoslovak Chemical Communications, 1959 , vol. 24, p. 1839,1840
反应条件
n-butyllithium; nickel Multistep reaction;
参考文献
Cabiddu, Salvatore; Fattuoni, Claudia; Floris, Costantino; Gelli, Gioanna; Melis, Stefana; Sotgiu, Francesca
Tetrahedron, 1990 , vol. 46, # 3 p. 861 - 884
反应条件
1: KMnO4, aq. NaOH 2: (i) SOCl2, THF, (ii) /BRN= 605268/, Et2O View Scheme
参考文献
Chodnekar; Blum
Journal of medicinal chemistry, 1968 , vol. 11, # 5 p. 1023 - 1028
反应条件
n-butyllithium; nickel Multistep reaction;
参考文献
Tetrahedron, , vol. 46, # 3 p. 861 - 884
