5,10-二氢-5,10-二甲基吩嗪合成路线 （共 10 条）
反应条件
ethylene glycol dimethyl ether
参考文献
Journal of the American Chemical Society, , vol. 79, p. 6178
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 304,309, 312
Chem.Abstr., , p. 9452
参考文献
Journal of the American Chemical Society, , vol. 104, # 26 p. 7581 - 7585
反应条件
n-butyllithium in ethylene glycol dimethyl ether; hexane 0.833333 h; Ambient temperature;
参考文献
Sugimoto, Akira; Kotani, Takeshi; Tsujimoto, Junko; Yoneda, Shigeo
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 435 - 438
反应条件
1: aqueous HCl 2: Lufteinwirkung View Scheme
参考文献
Journal of the Chemical Society, , p. 738,740
反应条件
1: aqueous HCl 2: Lufteinwirkung View Scheme
参考文献
Journal of the Chemical Society, , p. 738,740
反应条件
sodium acetate; acetic acid
参考文献
Journal of the Chemical Society, , p. 738,740
反应条件
hydrogen bromide; dimethyl sulfoxide T=100 - 110°C; oxidative demethylation; 2 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 36, # 4 p. 1057 - 1064
反应条件
1: 12 percent / HBr; DMSO / 2 h / 100 - 110 °C 2: 7 percent / HBr; DMSO / H2O / 2 h / 80 - 90 °C View Scheme
参考文献
Sugimoto, Akira; Yoshino, Yasuyuki; Watanabe, Ryo; Mizuno, Kazuhiko; Uehara, Kaku
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 4 p. 1057 - 1064
反应条件
1: 77 percent / HBr; DMSO / 2 h / 100 - 110 °C 2: 75 percent / nitrobenzene / 0.12 h / 100 °C View Scheme
参考文献
Sugimoto, Akira; Yoshino, Yasuyuki; Watanabe, Ryo; Mizuno, Kazuhiko; Uehara, Kaku
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 4 p. 1057 - 1064
反应条件
hydrogen bromide; dimethyl sulfoxide
T=100 - 110°C; oxidative demethylation; 2 h;
参考文献
Sugimoto, Akira; Yoshino, Yasuyuki; Watanabe, Ryo; Mizuno, Kazuhiko; Uehara, Kaku
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 4 p. 1057 - 1064
