3,6-二甲基-2-硝基苯胺合成路线 （共 7 条）
反应条件
sulfuric acid; nitric acid T=15 - 20°C; Erhitzen mit wss.HCl;
参考文献
van Helden et al.
Recueil des Travaux Chimiques des Pays-Bas, 1954 , vol. 73, p. 39,47
反应条件
sulfuric acid; nitric acid
参考文献
Noelting; Witt; Forel
Chemische Berichte, 1885 , vol. 18, p. 2667
反应条件
nitric acid verseift das hierbei erhaltene 5-Nitro-2-acetamino-p-xylol;
参考文献
Noelting; Witt; Forel
Chemische Berichte, 1885 , vol. 18, p. 2667
反应条件
palladium on activated charcoal 1.) nitration, 2.) toluene-EtOH; Yield given. Multistep reaction;
参考文献
Thulin, Bengt; Wennerstroem, Olof
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 7 p. 589 - 596
反应条件
hydrogen; palladium on activated charcoal in ethanol; toluene
参考文献
Thulin, Bengt; Wennerstroem, Olof
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 7 p. 589 - 596
反应条件
1: 51 percent / H2 / Pd/C / ethanol; toluene
2: 40 percent / NaNO2, conc. H2SO4, phosphoric acid, KI / 0 °C
3: 1.3 g / NBS, dibenzoyl peroxide / CCl4 / 24 h / Heating
View Scheme
参考文献
Thulin, Bengt; Wennerstroem, Olof
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 7 p. 589 - 596
反应条件
1: 51 percent / H2 / Pd/C / ethanol; toluene
2: 40 percent / NaNO2, conc. H2SO4, phosphoric acid, KI / 0 °C
View Scheme
参考文献
Thulin, Bengt; Wennerstroem, Olof
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 7 p. 589 - 596
