[Ru(tris(2,2'-bipyridyl))3](ClO4)2; triethanolamine; Ni((C6H5)CH2O)(C5H2N)(CH2)2(NHCH2CH2CH2)2NH(2+) in acetonitrile T=25°C; 3 h; Photolysis;

1: 1,3-dimethoxy benzene With n-butyllithium in tetrahydrofuran; hexane T=0 - 25°C; 5 h; Inert atmosphere; 2: 2,3-dibromo-1,4-dimethylbenzene in tetrahydrofuran; hexane T=0 - 25°C; Inert atmosphere;

[Ru(tris(2,2'-bipyridyl))3](ClO4)2; triethanolamine; Ni((C6H5)CH2O)(C5H2N)(CH2)2(NHCH2CH2CH2)2NH(2+) in acetonitrile T=25°C; 3 h; Photolysis;

n-butyllithium in tetrahydrofuran; hexane 1) -78 deg C, 2 h, 2) to RT;

<b>Multi-step reaction with 3 steps<br /> </b>1.1: isopropylmagnesium chloride / tetrahydrofuran / 3 h / -78 &deg;C / Inert atmosphere<br />1.2: -78 - 25 &deg;C / Inert atmosphere<br />2.1: isopropylmagnesium chloride lithium chloride complex / tetrahydrofuran / 2 h / -78 &deg;C / Inert atmosphere<br />2.2: -78 - 25 &deg;C / Inert atmosphere<br />3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol; water; toluene / 18 h / Inert atmosphere; Reflux<br /> <br /> &nbsp;