sodium hydroxide; tetracarbonylcobaltate(1-) ion in methanol T=55°C; 4 h;

potassium hydroxide in methanol; water T=60°C; 3 h;

暂无反应条件数据

hydrogenchloride; hydrogen sulfide in acetic acid

sodium hypochlorite; sodium chlorite; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical in aq. phosphate buffer; water; acetonitrile T=20 - 35°C; pH=6.7; 6 h; Inert atmosphere;

pyridine hydrochloride T=220°C; 1 h;

methyloxirane in water; acetonitrile 4 h; Irradiation;

1.1: potassium tert-butylate / tetrahydrofuran / 0.75 h / 0 °C / |Inert atmosphere 1.2: 1 h / 20 °C / |Inert atmosphere 2.1: 1,1,2,2-tetramethylethylene; potassium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol / 0.73 h / 20 °C View Scheme

1.1: 9-bora-bicyclo[3.3.1]nonane / toluene / 18 h / |Inert atmosphere; |Reflux 1.2: 2 h / 20 °C / |Inert atmosphere; |Reflux 2.1: sodium hydroxide; tetrakis(triphenylphosphine) palladium(0) / water; tetrahydrofuran / 16 h / |Inert atmosphere; |Reflux 3.1: 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; sodium chlorite; sodium hypochlorite / water; acetonitrile; aq. phosphate buffer / 6 h / 20 - 35 °C / pH 6.7 / |Inert atmosphere View Scheme

1: sodium hydroxide; tetrakis(triphenylphosphine) palladium(0) / water; tetrahydrofuran / 16 h / |Inert atmosphere; |Reflux 2: 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; sodium chlorite; sodium hypochlorite / water; acetonitrile; aq. phosphate buffer / 6 h / 20 - 35 °C / pH 6.7 / |Inert atmosphere View Scheme