2-(4-甲氧基苯基)-1-(2,4,6-三羟基苯基)乙酮合成路线 （共 20 条）
反应条件
hydrogenchloride; zinc(II) chloride in diethyl ether 1.) 0 deg C, 6 h, 2.) r.t., 24 h;
参考文献
Pelter, Andrew; Ward, Robert S.; Whalley, Jacqueline L.
Synthesis, 1998 , # 12 p. 1793 - 1802
反应条件
zinc(II) chloride; trichlorophosphate 24 h; Ambient temperature;
参考文献
Devi, Nirada; Jain, Niveta; Krishnamurty, H. G.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 8 p. 874 - 875
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Bulletin de la Societe Chimique de France, , p. 2309 - 2322
反应条件
aluminium trichloride; nitrobenzene
参考文献
Journal of Organic Chemistry, , vol. 10, p. 288,290
参考文献
Journal of Scientific and Industrial Research, , vol. 4, p. 231,234
Journal of Scientific and Industrial Research, , vol. 9 B, p. 25
反应条件
potassium carbonate; acetone Behandeln des Reaktionsprodukts mit wss. Natronlauge;
参考文献
Gilbert et al.
Journal of the Chemical Society, 1957 , p. 3740,3745
反应条件
1: N,N-dimethyl-formamide With phosphorus pentachloride T=55°C; Chlorination; 0.333333 h; 2: 2,4,6-trihydroxy-4'-methoxy deoxybenzoin With boron trifluoride diethyl etherate in N,N-dimethyl-formamide T=20°C; Cycloaddition; 1 h;
参考文献
Balasubramanian, Sreenivasan; Nair, Muraleedharan G.
Synthetic Communications, 2000 , vol. 30, # 3 p. 469 - 484
反应条件
4-(N,N-dimethlyamino)pyridine T=100°C; 4 h;
参考文献
Li, Wanmei; Liu, Fangming; Zhang, Pengfei
Journal of Chemical Research, 2008 , # 12 p. 683 - 685
反应条件
boron trifluoride diethyl etherate; acetic anhydride in diethyl ether; acetic acid Heating;
参考文献
Jah, Hem Chandra; Zilliken, Fritz; Breitmaier, Eberhard
Angewandte Chemie, 1981 , vol. 93, # 1 p. 129 - 130
反应条件
1: 2,4,6-trihydroxy-4'-methoxy deoxybenzoin With boron trifluoride diethyl etherate in N,N-dimethyl-formamide T=10°C; 2: methanesulfonyl chloride in N,N-dimethyl-formamide T=10 - 55°C;
参考文献
Chen, Xiang; Tang, Li-Jun; Sun, Yu-Na; Qiu, Pei-Hong; Liang, Guang
Journal of Inorganic Biochemistry, 2010 , vol. 104, # 4 p. 379 - 384
