2-三氟甲基-4-硝基苯酚合成路线 （共 15 条）
反应条件
lithium chloride in N,N-dimethyl-formamide 3 h; Inert atmosphereReflux;
参考文献
Yang, Hong; Wang, Lixing; Shao, Renfan; Clark, Noel A.; Ortega, Josu; Etxebarria, Jesus; Albouy, Pierre-Antoine; Walba, David M.; Keller, Patrick
Journal of Materials Chemistry, 2009 , vol. 19, # 39 p. 7208 - 7215
反应条件
sodium hydroxide in dimethyl sulfoxide T=25°C; 8 h;
参考文献
CHANG GUNG UNIVERSITY; TSENG, CHING-PING; HSIEH, PEI-WEN; CHANG, YAO-WEN
Patent: US2014/11882 A1, 2014 ;
Location in patent: Paragraph 0009; 0029 ;
反应条件
1: With copper(l) iodide; 1,10-phenanthroline; potassium hydroxide in water; dimethyl sulfoxide T=20 - 100°C; Inert atmosphere; 2: With hydrogenchloride in water; dimethyl sulfoxide T=20°C; Inert atmosphere;
参考文献
Zhao, Dongbing; Wu, Ningjie; Zhang, Shuai; Xi, Peihua; Su, Xiaoyu; Lan, Jingbo; You, Jingsong
Angewandte Chemie - International Edition, 2009 , vol. 48, # 46 p. 8729 - 8732
反应条件
tert.-butylhydroperoxide; potassium tert-butylate; ammonia in tetrahydrofuran 0.25 h;
参考文献
Makosza, Mieczyslaw; Sienkiewicz, Krzysztof
Journal of Organic Chemistry, 1998 , vol. 63, # 13 p. 4199 - 4208
反应条件
triethylamine in water; acetonitrile T=25°C; 7 h; Kinetics; Reagent/catalyst;
参考文献
Cho, Bong Rae; Pyun, Sang Yong
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 4 p. 1030 - 1034
反应条件
hydrogen bromide in water; acetic acid 96 h; Heating / reflux;
参考文献
US2005/96337 A1, ;
Page/Page column 35 ;
反应条件
aqueous nitric acid in water; ethyl acetate; Petroleum ether
参考文献
US5254677 A1, ;
US 5254677 A
参考文献
Sankyo Company, Limited
Patent: US6555556 B1, 2003 ;
US 6555556 B1
反应条件
1: With sulfuric acid; sodium nitrite 1 h; 2: With water T=100°C; 65 h; Cooling with ice; 3: With ammonia in water T=20°C;
参考文献
Udagawa, Chikako; Fukuyoshi, Shuichi; Morimoto, Shotaro; Tanimoto, Yoshifumi; Nakagaki, Ryoichi
Journal of Photochemistry and Photobiology A: Chemistry, 2011 , vol. 226, # 1 p. 57 - 63
反应条件
tetramethyl-ammonium fluoride in N,N-dimethyl acetamide T=60°C;
参考文献
Tetrahedron Letters, , vol. 34, # 24 p. 3901 - 3902
