1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; Inert atmosphereSealed tube; 2: With 1,2,2-trichloro-1,1,2-trichloro-ethane in tetrahydrofuran; hexane T=-78°C; Inert atmosphere;
参考文献
RUTGERS, THE STATE UNIVERSITY OF NEW JERSEY
Patent: US2011/282067 A1, 2011 ;
Location in patent: Page/Page column 2-3 ;
