反应条件
1: 64 percent / tri-N-methylanilinium perbromide / tetrahydrofuran / 1) 15 min, 0 deg C, 2) 15 min, rt 2: 90 percent / LiHCO3, LiBr / dimethylformamide / 0.5 h / Heating 3: 60 percent / H2, quinoline / 5percent Pd/CaCO3 / ethanol / 0.27 h / 760 Torr / Ambient temperature 4: 72 percent / H2, 0.1 N NaOH / 5percent Pd/C / ethanol / 2 h / 760 Torr / Ambient temperature View Scheme
参考文献
Dolle; Hetru; Roussel; Rousseau; Sobrio; Luu; Hoffmann
Tetrahedron, 1991 , vol. 47, # 34 p. 7067 - 7080
