3,3＇-二硫代二丙酸二甲酯合成路线 （共 17 条）
反应条件
sodium sulfite in water T=10°C; 24 h; Inert atmosphere; Product distribution / selectivity;
参考文献
SK Chemicals Co., Ltd.
Patent: US2012/330061 A1, 2012 ;
Location in patent: Page/Page column 7 ;
反应条件
hydrogen sulfide; sodium sulfite in water T=50 - 55°C; P=760.051 Torr; 10.25 h; ConcentrationTemperatureReagent/catalystTime;
参考文献
Beijing Tianqing Chemicals Co., Ltd.; XIAO, Haihuan; ZHANG, Xiaolin; JIN, Yuechun
Patent: EP2684869 A1, 2014 ;
Location in patent: Paragraph 0030 ;
反应条件
dilithium tetrachloropalladate in methanol 16 h; Ambient temperature;
参考文献
Bergstrom, Donald E.; Beal, Peter; Jenson, Jeffrey; Lin, Xiaoping
Journal of Organic Chemistry, 1991 , vol. 56, # 19 p. 5598 - 5602
反应条件
potassium hydride in N,N-dimethyl-formamide
T=20°C; Alkylation; 1 h;
参考文献
Hamel, Pierre; Girard, Mario
Journal of Organic Chemistry, 2000 , vol. 65, # 10 p. 3123 - 3125
反应条件
potassium hydride in N,N-dimethyl-formamide
T=20°C; Alkylation; 18 h;
参考文献
Hamel, Pierre; Girard, Mario
Journal of Organic Chemistry, 2000 , vol. 65, # 10 p. 3123 - 3125
反应条件
hydrazine hydrate in methanol
T=20°C;
参考文献
Rodriguez-Docampo, Zaida; Otto, Sijbren
Chemical Communications, 2008 , # 42 p. 5301 - 5303
反应条件
chlorine in dichloromethane
T=-35°C; 0.5 h;
参考文献
Hamel, Pierre; Girard, Mario
Journal of Organic Chemistry, 2000 , vol. 65, # 10 p. 3123 - 3125
