N-苯基苯羰基亚肼酰氯合成路线 (共 129 条)
反应条件
phosphorus pentachloride
参考文献
Wyrebek, Przemyslaw; Ostrowski, Stanislaw
Bulletin of the Chemical Society of Japan, 2012 , vol. 85, # 10 p. 1167 - 1174,8
反应条件
N-chlorosuccinimide-dimethyl sulfide in dichloromethane T=-40°C; 0.5 h;
参考文献
Patel, Himatkumar V.; Vyas, Kavita A.; Pandey, Sudhanshu P.; Fernandes, Peter S.
Tetrahedron, 1996 , vol. 52, # 2 p. 661 - 668
反应条件
CuCl2*2H2O in acetone T=0°C; 1 h;
参考文献
Attanasi, Orazio; Battistoni, Paolo; Fava, Gabriele
Canadian Journal of Chemistry, 1983 , vol. 61, p. 2665 - 2668
反应条件
1: toluene / 12 h / 20 °C 2: N-chloro-succinimide; dimethylsulfide / dichloromethane / -78 - 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 52, # 48 p. 6372 - 6375
反应条件
triethylamine in dichloromethane T=-40°C; 0.5 h; other substituted hydrazones; also without Et3N; Mechanism;
参考文献
Patel, Himatkumar V.; Vyas, Kavita A.; Pandey, Sudhanshu P.; Fernandes, Peter S.
Tetrahedron, 1996 , vol. 52, # 2 p. 661 - 668
反应条件
1: toluene / 12 h / 20 °C 2: N-chloro-succinimide; dimethylsulfide / dichloromethane / -78 - 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 52, # 48 p. 6372 - 6375
反应条件
1: triethylamine / diethyl ether / 0 °C 2: phosphorus pentachloride / diethyl ether / 1.5 h / 20 °C / |Reflux View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 85, # 10 p. 1167 - 1174,8
反应条件
phosphorus pentachloride 1.) CCl4, reflux, 3 h; 2.) CCl4, 0 deg C, 1 h; Yield given. Multistep reaction;
参考文献
European Journal of Medicinal Chemistry, , vol. 22, p. 147 - 152
反应条件
Reaktion mit:Produkt 5: Benzoesaeure-<N'-(2-oxo-3,5-diphenyl-2,3-dihydro-2λ5-<1,3,4,2>oxadiazaphosphol-2-yl)-N'-phenyl-hydrazid>.;
参考文献
Chemische Berichte, , vol. 27, p. 322
Chemische Berichte, , vol. 27, p. 2121,2123
反应条件
triethylamine in tetrahydrofuran 70 h; Heating;
参考文献
Bojilova, Anka; Rodios, Nestor A.; Alexandrou, Nicholas E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3233 - 3238