3-正-丁基-2,4-戊烷二酮合成路线 （共 32 条）
反应条件
1: 1.) zinc, sodium acetate / 1.) acetic acid, 80 deg C, 40 min; 2.) acetic acid, 20 min, 95-105 deg C
2: 67 percent / sodium / 4 h / 80 °C / 15 Torr
View Scheme
参考文献
Lecas-Nawrocka, Alexandra; Levisalles, Jacques; Mariacher, Claire; Renko, Zafiarisoa; Rose, Eric
Canadian Journal of Chemistry, 1984 , vol. 62, p. 2054 - 2058
反应条件
1: 1.) t-BuOK / 1.) Me2SO, room temp., 2.) Me2SO, irradiation, room temp., 6 h
2: 74 percent / lithium salt of 2-nitropropane / hexamethylphosphoric acid triamide / 5 h / Ambient temperature; Irradiation
View Scheme
参考文献
Ono, Noboru; Tamura, Rui; Eto, Hiromichi; Hamamoto, Isami; Nakatsuka, Tamon; et al.
Journal of Organic Chemistry, 1983 , vol. 48, # 21 p. 3678 - 3684
