反应条件
1: 3-chloro-1-(p-toluenesulfonyl)pyrrole With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; Metallation; 1.25 h;
2: N,N-dimethyl-formamide in tetrahydrofuran
T=-78°C; Formylation; detosylation; 1 h;
参考文献
Robertson, Jeremy; Kuhnert, Nikolai; Zhao, Yuekun
Heterocycles, 2000 , vol. 53, # 11 p. 2415 - 2420