1,3-联苯-1-丁酮合成路线 (共 114 条)
反应条件
tri-tert-butyl phosphine; bis(.eta.(2)-ethylene)(2,4,-pentanedionato)rhodium in 1,4-dioxane T=100°C; 16 h;
参考文献
Matsuda, Takanori; Makino, Masaomi; Murakami, Masahiro
Bulletin of the Chemical Society of Japan, 2005 , vol. 78, # 8 p. 1528 - 1533
反应条件
InI3; trimethylsilyl iodide in dichloromethane T=20°C; 2 h; Inert atmosphere;
参考文献
Onishi, Yoshiharu; Nishimoto, Yoshihiro; Yasuda, Makoto; Baba, Akio
Chemistry Letters, 2011 , vol. 40, # 11 p. 1223 - 1225
反应条件
silver trifluoromethanesulfonate in dichloromethane 2 h; Ambient temperature;
参考文献
Takeda, Kazuyoshi; Torii, Katsumi; Ogura, Haruo
Tetrahedron Letters, 1990 , vol. 31, # 2 p. 265 - 266
反应条件
in tetrahydrofuran T=-78°C;
参考文献
Nagashima, Hideo; Ozaki, Nobuyasu; Washiyama, Masayoshi; Itoh, Kenji
Tetrahedron Letters, 1985 , vol. 26, # 5 p. 657 - 660
反应条件
in toluene T=80°C; 4 h;
参考文献
Synthesis, , # 9 p. 1127 - 1130
反应条件
in diethyl ether T=0°C;
参考文献
Fleming, Ian; Lewis, Jeremy J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3257 - 3266
反应条件
anhydrous iron chloride in 1,2-dichloro-ethane T=60°C; 3 h; regioselective reaction;
参考文献
Yang, Cui-Feng; Wang, Jian-Yong; Tian, Shi-Kai
Chemical Communications, 2011 , vol. 47, # 29 p. 8343 - 8345
反应条件
[Rh(OH)(cycloocta-1,5-diene)]2; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in methanol T=50°C; Inert atmosphere;
参考文献
Organic Letters, , vol. 15, # 13 p. 3226 - 3229
反应条件
diethyl ether; manganese (II) chloride T=0 - 5°C;
参考文献
Journal of the American Chemical Society, , vol. 64, p. 2972,2975
反应条件
aluminium trichloride in 1,2-dichloro-benzene 5 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 71, # 11 p. 4312 - 4315