1,3-联苯-1-丁酮合成路线 （共 114 条）
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; trichlorosilane in dichloromethane T=0 - 20°C; 24 h; Inert atmosphere;
参考文献
Sugiura, Masaharu; Sato, Norimasa; Kotani, Shunsuke; Nakajima, Makoto
Chemical Communications, 2008 , # 36 p. 4309 - 4311
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; caesium carbonate in toluene T=100°C; 15 h; Inert atmosphere;
参考文献
Bizet, Vincent; Pannecoucke, Xavier; Renaud, Jean-Luc; Cahard, Dominique
Journal of Fluorine Chemistry, 2013 , vol. 152, p. 56 - 61
反应条件
1: Bromure de phenyl magnesium With indium(III) chloride in tetrahydrofuran T=20°C; 0.5 h; 2: With water in tetrahydrofuran T=20°C; 0.166667 h; 3: 1-phenyl-2-buten-1-one With [Rh(OH)(cycloocta-1,5-diene)]2 in tetrahydrofuran T=20°C; 6 h;
参考文献
Miura, Tomoya; Murakami, Masahiro
Chemical Communications, 2005 , # 45 p. 5676 - 5677
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; caesium carbonate in toluene T=100°C; 15 h; Inert atmosphere;
参考文献
Bizet, Vincent; Pannecoucke, Xavier; Renaud, Jean-Luc; Cahard, Dominique
Journal of Fluorine Chemistry, 2013 , vol. 152, p. 56 - 61
反应条件
3β,17β-dihydroxy-17α-methylandrost-5-ene in diethyl ether; hexane; toluene T=-78°C;
参考文献
Tetrahedron Letters, , vol. 28, # 46 p. 5723 - 5726
反应条件
1: With gallium(III) bromide in 1,2-dichloro-ethane T=83°C; 2 h; Inert atmosphere; 2: With sodium hydrogencarbonate in diethyl ether; water; 1,2-dichloro-ethane
参考文献
Nishimoto, Yoshihiro; Onishi, Yoshiharu; Yasuda, Makoto; Baba, Akio
Angewandte Chemie - International Edition, 2009 , vol. 48, # 48 p. 9131 - 9134
反应条件
tetrabutyl ammonium fluoride; antimony trichloride; acetic acid; palladium diacetate in acetonitrile T=60°C; 41 h;
参考文献
Denmark, Scott E.; Amishiro, Nobuyoshi
Journal of Organic Chemistry, 2003 , vol. 68, # 18 p. 6997 - 7003
反应条件
bis(.eta.(2)-ethylene)(2,4,-pentanedionato)rhodium; tri-tert-butyl phosphine; caesium carbonate in 1,4-dioxane T=100°C; 24 h;
参考文献
Matsuda, Takanori; Makino, Masaomi; Murakami, Masahiro
Organic Letters, 2004 , vol. 6, # 8 p. 1257 - 1259
反应条件
indium(III) chloride in dichloromethane T=20°C; 2 h;
参考文献
Nishimoto, Yoshihiro; Yasuda, Makoto; Baba, Akio
Organic Letters, 2007 , vol. 9, # 24 p. 4931 - 4934
反应条件
potassium hydroxide; dipotassium tetrachloroplatinate in 1,4-dioxane T=70°C; 1 h;
参考文献
Hayashi, Tamio; Sasaki, Keigo
Chemistry Letters, 2008 , vol. 37, # 8 p. 842 - 843
