(2-甲基苄基)三苯基溴化膦合成路线 （共 9 条）
反应条件
in acetonitrile Reflux;
参考文献
Matsumoto, Kouichi; Fujie, Shunsuke; Suga, Seiji; Nokami, Toshiki; Yoshida, Jun-Ichi
Chemical Communications, 2009 , # 36 p. 5448 - 5450
参考文献
Yamataka, Hiroshi; Nagareda, Katsushi; Ando, Katsuhiro; Hanafusa, Terukiyo
Journal of Organic Chemistry, 1992 , vol. 57, # 10 p. 2865 - 2869
反应条件
n-butyllithium 1.) THF, hexane, 0 deg C, 1 h, 2.) THF, hexane, -78 deg C to rt, 3 h; Yield givenMultistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Lawrence, Nicholas J.; Muhammad, Faiz
Tetrahedron, 1998 , vol. 54, # 50 p. 15361 - 15370
参考文献
Lawrence, Nicholas J.; Muhammad, Faiz
Tetrahedron Letters, 1994 , vol. 35, # 32 p. 5903 - 5906
反应条件
potassium tert-butylate in N,N-dimethyl-formamide
参考文献
Chess, Edward K.; Lin, Ping-Huang; Gross, Michael L.
Journal of Organic Chemistry, 1983 , vol. 48, # 9 p. 1522 - 1527
反应条件
(i) nBuLi, (ii) air; Multistep reaction;
参考文献
Seyferth,D. et al.
Journal of the American Chemical Society, 1975 , vol. 97, # 26 p. 7417 - 7426
反应条件
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Shi, Yian
Patent: US6348608 B1, 2002 ;
Location in patent: Page column 29 ;
反应条件
1: (i) nBuLi, (ii) /BRN= 606301/
2: Py*HBr3, AcOH
3: KOH, triethylene glycol / 160 °C
View Scheme
参考文献
Gust,D.
Journal of the American Chemical Society, 1977 , vol. 99, # 21 p. 6980 - 6982
反应条件
1: (i) nBuLi, (ii) air
2: (bromination)
3: KOH
View Scheme
参考文献
Seyferth,D. et al.
Journal of the American Chemical Society, 1975 , vol. 97, # 26 p. 7417 - 7426
