(3,3-二甲基烯丙基)三苯基溴化膦合成路线 （共 11 条）
反应条件
in toluene T=110°C; Inert atmosphere;
参考文献
Coulombel, Lydie; Weiwer, Michel; Dunach, Elisabet
European Journal of Organic Chemistry, 2009 , # 33 p. 5788 - 5795
反应条件
sodium bromide; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; methanol 2 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 57, # 10 p. 3013 - 3014
反应条件
1: 11 g / hydrobromic acid / 8 h / 0 °C 2: 27.2 g / benzene / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 8 p. 2182 - 2187
反应条件
in 1,3,5-trimethyl-benzene Heating;
参考文献
Journal of Organic Chemistry, , vol. 36, p. 4033 - 4041
参考文献
Journal of Organic Chemistry, , vol. 40, p. 1294 - 1298
反应条件
in methanol 96 h; Ambient temperature;
参考文献
Bulletin de la Societe Chimique de France, , p. 1298 - 1302
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 48, # 4 p. 897 - 902,818 - 822
反应条件
lithium ethanolate in N,N-dimethyl-formamide T=-90°C; 20 h;
参考文献
Journal of Chemical Research, Miniprint, , # 3 p. 826 - 852
反应条件
n-butyllithium in tetrahydrofuran; hexane 1 h; Ambient temperature;
参考文献
Tzirakis, Manolis D.; Alberti, Mariza N.; Orfanopoulos, Michael
Organic Letters, 2011 , vol. 13, # 13 p. 3364 - 3367
反应条件
n-butyllithium
1.) THF, hexane, 25 deg C, 2 h, 2.) 25 deg C, 24 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tamura, Rui; Saegusa, Koji; Kakihana, Masato; Oda, Daihei
Journal of Organic Chemistry, 1988 , vol. 53, # 12 p. 2723 - 2728
